Reference Material
This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO 9001.
Product Name(产品名称) 78 Pesticide Mix in Acetonitrile(乙腈中78种农药混标)
Storage(存储条件) (-18±5)℃
Transportation(运输条件) Biological ice bag transportation (生物冰袋运输)
|
CERTIFIED
|
Component
No.
(组分数)
|
Peak
Sequence
(出峰顺序)
|
Component
(组分)
|
CAS No.
|
Concentration
(μg/mL)
(浓度)
|
Relative Expanded
Uncertainty(%) (k=2)
(相对扩展不确定度)
|
|
1
|
1
|
Oxamyl-oxime (杀线威-oxime)
|
30558-43-1
|
100
|
3
|
|
2
|
2
|
Aldicarb Sulfoxide (涕灭威亚砜)
|
1646-87-3
|
100
|
3
|
|
3
|
3
|
Aldicarb-sulfone (涕灭威砜)
|
1646-88-4
|
100
|
3
|
|
4
|
4
|
Nitenpyram (E-烯啶虫胺)
|
150824-47-8
|
100
|
3
|
|
5
|
5
|
Oxamyl (杀线威)
|
23135-22-0
|
100
|
3
|
|
6
|
6
|
Methomyl (灭多威)
|
16752-77-5
|
100
|
3
|
|
7
|
7
|
Flonicamid (氟啶虫酰胺)
|
158062-67-0
|
100
|
3
|
|
8
|
8
|
Thiamethoxam (噻虫嗪)
|
153719-23-4
|
100
|
3
|
|
9
|
9
|
Carbendazim (多菌灵)
|
10605-21-7
|
100
|
3
|
|
10
|
10
|
Methiocarb Sulfoxide (甲硫威亚砜)
|
2635-10-1
|
100
|
3
|
|
11
|
11
|
Desmethyl-pirimicarb (脱甲基抗蚜威)
|
30614-22-3
|
100
|
3
|
|
12
|
12
|
Carbofuran-3-hydroxy (3-羟基呋喃丹)
|
16655-82-6
|
100
|
3
|
|
13
|
13
|
Cymoxanil (霜脲氰)
|
57966-95-7
|
100
|
3
|
|
14
|
14
|
Aldicarb (涕灭威)
|
116-06-3
|
100
|
3
|
|
15
|
15
|
Florasulam (双氟磺草胺)
|
145701-23-1
|
100
|
3
|
|
16
|
16
|
Metolcarb (速灭威)
|
1129-41-5
|
100
|
3
|
|
17
|
17
|
Propoxur (残杀威)
|
114-26-1
|
100
|
3
|
|
18
|
18
|
Carbofuran (克百威)
|
1563-66-2
|
100
|
3
|
|
19
|
19
|
Bendiocarb (恶虫威)
|
22781-23-3
|
100
|
3
|
|
20
|
20
|
Thiophanate-methyl (甲基硫菌灵)
|
23564-05-8
|
100
|
3
|
|
21
|
21
|
Carbaryl (甲萘威)
|
63-25-2
|
100
|
3
|
|
22
|
22
|
Cyantraniliprole (溴氰虫酰胺)
|
736994-63-1
|
100
|
3
|
|
23
|
23
|
Isoprocarb (异丙威)
|
2631-40-5
|
100
|
3
|
|
24
|
24
|
Isoproturon (异丙隆)
|
34123-59-6
|
100
|
3
|
|
25
|
25
|
Metalaxyl (甲霜灵)
|
57837-19-1
|
100
|
3
|
|
26
|
26
|
Benazolin-ethyl Ester (草除灵乙酯)
|
25059-80-7
|
100
|
3
|
|
27
|
27
|
Fenobucarb (仲丁威)
|
3766-81-2
|
100
|
3
|
|
28
|
28
|
Chlorantraniliprole (氯虫苯甲酰胺)
|
500008-45-7
|
100
|
3
|
|
29
|
29
|
Phenmedipham (甜菜宁)
|
13684-63-4
|
100
|
3
|
|
30
|
30
|
Diethofencarb (乙霉威)
|
87130-20-9
|
100
|
3
|
|
31
|
31
|
Methiocarb (甲硫威)
|
2032-65-7
|
100
|
3
|
|
32
|
32
|
Fenamidone (咪唑菌酮)
|
161326-34-7
|
100
|
3
|
|
33
|
33
|
Promecarb (猛杀威)
|
2631-37-0
|
100
|
3
|
|
34
|
34
|
Ethiprole (乙虫腈)
|
181587-01-9
|
100
|
3
|
|
35
|
35
|
Procymidone (腐霉利)
|
32809-16-8
|
100
|
3
|
|
36
|
36
|
Fenpyrazamine (胺苯吡菌酮)
|
473798-59-3
|
100
|
3
|
|
37
|
37
|
Iprovalicarb1 (缬霉威)
|
140923-17-7
|
100
|
3
|
|
38
|
38
|
Fenothiocarb (苯硫威)
|
62850-32-2
|
100
|
3
|
|
39
|
39
|
Iprodione (异菌脲)
|
36734-19-7
|
100
|
3
|
|
40
|
40
|
Diflubenzuron (除虫脲)
|
35367-38-5
|
100
|
3
|
|
41
|
41
|
Fenoxycarb (苯氧威)
|
72490-01-8
|
100
|
3
|
|
42
|
42
|
Kresoxim-methyl (醚菌酯)
|
143390-89-0
|
100
|
3
|
|
43
|
43
|
Carfentrazone-ethyl (氟酮唑草)
|
128639-02-1
|
100
|
3
|
|
44
|
44
|
Prochloraz Desimidazole-formylamino ( 咪鲜胺-脱咪唑甲酰氨基)
|
139542-32-8
|
100
|
3
|
|
45
|
45
|
Prochloraz-desimidazole-amino (咪鲜胺-脱氨基咪唑)
|
139520-94-8
|
100
|
3
|
|
46
|
46
|
Prochloraz (咪鲜胺)
|
67747-09-5
|
100
|
3
|
|
47
|
47
|
Pyraflufen-ethyl (吡草醚)
|
129630-19-9
|
100
|
3
|
|
48
|
48
|
Oxadiargyl (丙炔噁草酮)
|
39807-15-3
|
100
|
3
|
|
49
|
49
|
Triflumuron (杀铃脲)
|
64628-44-0
|
100
|
3
|
|
50
|
50
|
Bifenox (甲羧除草醚)
|
42576-02-3
|
100
|
3
|
|
51
|
51
|
Trifloxystrobin (肟菌酯)
|
141517-21-7
|
100
|
3
|
|
52
|
52
|
Indoxacarb (茚虫威)
|
144171-61-9
|
100
|
3
|
|
53
|
53
|
Amisulbrom (吲唑磺菌胺)
|
348635-87-0
|
100
|
3
|
|
54
|
54
|
Hexaflumuron (氟铃脲)
|
86479-06-3
|
100
|
3
|
|
55
|
55
|
Novaluron (双苯氟脲)
|
116714-46-6
|
100
|
3
|
|
56
|
56
|
Diclofop-methyl (禾草灵-甲基)
|
51338-27-3
|
100
|
3
|
|
57
|
57
|
Furathiocarb (呋线威)
|
65907-30-4
|
100
|
3
|
|
58
|
58
|
Teflubenzuron (氟苯脲)
|
83121-18-0
|
100
|
3
|
|
59
|
59
|
Oxadiazon (恶草酮)
|
19666-30-9
|
100
|
3
|
|
60
|
60
|
Triallate (野麦畏)
|
2303-17-5
|
100
|
3
|
|
61
|
61
|
Flucythrinate (氟氰戊菊酯)
|
70124-77-5
|
100
|
3
|
|
62
|
62
|
Spiromesifen (螺甲螨酯)
|
283594-90-1
|
100
|
3
|
|
63
|
63
|
Flufenoxuron (氟虫脲)
|
101463-69-8
|
100
|
3
|
|
64
|
64
|
Propargite (炔螨特)
|
2312-35-8
|
100
|
3
|
|
65
|
65
|
Fenpropathrin (甲氰菊酯)
|
39515-41-8
|
100
|
3
|
|
66
|
66
|
Spirodiclofen (螺螨酯)
|
148477-71-8
|
100
|
3
|
|
67
|
67
|
Deltamethrin (溴氰菊酯)
|
52918-63-5
|
100
|
3
|
|
68
|
68
|
Fenvalerate (氰戊菊酯)
|
51630-58-1
|
100
|
3
|
|
69
|
69
|
Tau-fluvalinate (氟胺氰菊酯)
|
102851-06-9
|
100
|
3
|
|
70
|
70
|
Bioresmethrin (生物苄呋菊酯)
|
28434-01-7
|
100
|
3
|
|
71
|
71
|
Permethrin2 (氯菊酯)
|
52645-53-1
|
100
|
3
|
|
72
|
72
|
Etofenprox (醚菊酯)
|
80844-07-1
|
100
|
3
|
|
73
|
73
|
Bifenthrin (联苯菊酯)
|
82657-04-3
|
100
|
3
|
|
74
|
74
|
Fipronil Desulfinyl (氟甲腈)
|
205650-65-3
|
100
|
3
|
|
75
|
75
|
Fipronil (氟虫腈)
|
120068-37-3
|
100
|
3
|
|
76
|
76
|
Fipronil Sulfide (氟虫腈硫化物)
|
120067-83-6
|
100
|
3
|
|
77
|
77
|
Fipronil-sulfone (氟虫腈砜)
|
120068-36-2
|
100
|
3
|
|
78
|
78
|
Fluazinam (氟啶胺)
|
79622-59-6
|
100
|
3
|
Note
See the attachment below for the MRM mode.(关于MRM模式，请参阅下面的附件)
1.Iprovalicarb (CAS No. : 140923-17-7) has two peaks,the retention times are 15.524min and 15.759min.(缬霉威 (CAS No. : 140923-17-7)出两个峰，保留时间分别为：15.524min 和 15.759min)
2.Permethrin (CAS No. : 52645-53-1) has two peaks,the retention times are 20.662min and 20.924min.( 氯菊酯 (CAS No. : 52645-53-1)出两个峰，保留时间分别为：20.662min 和 20.924min)
3.Fipronil Desulfinyl (CAS No. : 205650-65-3),Fipronil (CAS No. : 120068-37-3),Fipronil Sulfide (CAS No. : 120067-83-6),Fipronil-sulfone (CAS No. : 120068-36-2) and Fluazinam (CAS No. : 79622-59-6) were dectected by LC-MS/MS with negative ion mode.( 氟甲腈 (CAS No. : 205650-65-3) ,氟虫腈(CAS No. : 120068-37-3),氟虫腈硫化物 (CAS No. : 120067-83-6),氟虫腈砜(CAS No. : 120068-36-2)和氟啶胺(CAS No. : 79622-59-6) 采用LC-MS/MS负离子模式检测)
4.The product contains a few of 0.1mol/L HCl.（本品含少量0.1mol/L盐酸。）